Determining the uncertainty in measurements involves several systematic steps to ensure accuracy and reliability. Here’s a detailed outline of the steps involved in uncertainty calculations:
Steps in Uncertainty Calculations
1. Define the Measurement Process
Clearly define what is being measured and the conditions under which the measurements are made.
Specify the instruments and techniques used for the measurement.
List all potential sources of uncertainty that might affect the measurement. These can include:
Instrument resolution
Calibration uncertainty
Environmental conditions
Measurement procedure
Operator influence
Drift over time
3. Quantify Individual Uncertainties
Manufacturer Specifications: Refer to the instrument’s manual or data sheet to find the specified uncertainties.
Calibration Data: Use uncertainties provided in the calibration certificate of the instrument.
Experimental Data: Conduct repeated measurements and statistical analysis to determine the standard deviation (repeatability).
Environmental Effects: Evaluate the influence of environmental conditions on the measurement.
4. Convert Uncertainties to Standard Uncertainties
If uncertainties are not already given as standard deviations, convert them. For example:
For a rectangular distribution (e.g., resolution), the standard uncertainty is the half-width divided by the square root of 3:
For a triangular distribution, the standard uncertainty is the half-width divided by the square root of 6:
5. Combine Standard Uncertainties
Combine the individual standard uncertainties using the root sum of squares (RSS) method to find the combined standard uncertainty (ucu):
6. Determine the Expanded Uncertainty
Multiply the combined standard uncertainty by a coverage factor (k) to obtain the expanded uncertainty (U).
The coverage factor depends on the desired confidence level (e.g., k=2k for approximately 95% confidence):
U=k⋅uc
7. Report the Uncertainty
Report the measurement result along with the expanded uncertainty and the confidence level.
For example: Measured value at 95% confidence level
Example Calculation for Pressure Measurement
Measurement Process:
Measuring pressure using a digital pressure gauge.
Conditions: room temperature, stable environment.
Identify Sources of Uncertainty:
Instrument resolution: ±0.1 kPa
Calibration uncertainty: ±0.2 kPa
Environmental factors: ±0.05 kPa
Repeatability (standard deviation from repeated measurements): ±0.1 kPa
Quantify Individual Uncertainties:
Instrument resolution (U1)
Calibration uncertainty (U2)
Environmental factors (U4)
Repeatability (U5)
Combine Standard Uncertainties, Uc= U1 + U2,+ U2+……+Un
Determine the Expanded Uncertainty:
Identify the Sources of Uncertainty
For both pressure and temperature measurement devices, uncertainties can arise from several sources, including:
Instrument Resolution: The smallest change that can be detected by the instrument.
Calibration: Uncertainties associated with the calibration process.
Environmental Factors: Temperature, humidity, and other environmental conditions affecting the measurement.
Drift: Changes in the instrument’s performance over time.
Measurement Procedure: Variations introduced by the method of measurement.
Operator Influence: Differences in how different operators use the instrument.
Quantify Each Source of Uncertainty
Each identified source of uncertainty needs to be quantified, usually in terms of a standard deviation. This can be done through:
Manufacturer Specifications: Use the instrument’s data sheet to find specified uncertainties.
Calibration Certificates: Refer to the calibration certificate for uncertainties associated with the calibration process.
Repeatability Studies: Perform repeated measurements to assess the repeatability of the instrument.
3. Combine the Uncertainties
Combine the individual uncertainties to obtain the overall uncertainty using the root sum of squares (RSS) method.
The combined standard uncertainty (ucu_cuc) is given by:
Formula for Uncertainty calculations
Expanded Uncertainty
To express the uncertainty with a higher level of confidence, calculate the expanded uncertainty (U) by multiplying the combined standard uncertainty by a coverage factor (kkk), typically 2 for a 95% confidence level.
U=k⋅uc
Example of Pressure Measurement Device
Instrument Resolution: ±0.1 kPa
Calibration Uncertainty: ±0.2 kPa
Environmental Factors: ±0.05 kPa
Repeatability: ±0.1 kPa
Combined Standard Uncertainty: U=2*0.25=0.5 kPa
Examples of Pressure Uncertainty calculations
Type of pressure measurement methods
Example of Temperature Measurement Device
Instrument Resolution: ±0.1°C
Calibration Uncertainty: ±0.15°C
Environmental Factors: ±0.05°C
Repeatability: ±0.1°C
Combined Standard Uncertainty:U=2*0.212=0.424°C
Examples of Temperature Uncertainty calculations
Temperature measurement Devices and its Types
Conclusion
By following these steps, you can determine the uncertainty of pressure and temperature measurement devices, providing a quantifiable measure of the confidence in your measurements
Reference
Michalski et al, Estimating uncertainty of temperature measurements